1H,15N HSQC spectra of Nsp3b: 600 μM of U-15N labeled Nsp3b (25 mM Bis-Tris pH 6.5, 150 mM NaCl, 3 mM TCEP and 5% D2O) measured at 298 K on a 1.2 GHz spectrometer with chemical shift assignment depicted and deposited at the BMRB (doi:10.13018/BMR50388)
1H,15N TROSY-HSQC spectra of Nsp3b ADPr: 300 μM of U-13C15N labeled Nsp3b (25 mM Bis-Tris pH 6.5, 150 mM NaCl, 3 mM TCEP, 6 mM ADPr and 5% D2O and 5% D2O) measured at 298 K on a 1.2 GHz Spectrometer with chemical shift assignment depicted and deposited at the BMRB (doi:10.13018/BMR50387)
Reference: Cantini, F. (2020) Biomol. NMR Assign. 14:339–346; Altincekic (2021) Front. Mol. Biosci.